Is there a library of pulse programs for the Bruker WM-360 on the net
somewhere? We are using a WM-360 (360MHz for 1H) with a widebore magnet
upgraded to Aspect 3000, running DISNMR.
Also:
As an organic chemist (I'm trained in interpretation, and only recently have
been put in total charge of the WM; maintenance, cryogens, programming, etc.)
I'm a little worried about arcing the probe. I've heard many stories about it.
We just purchased a H-C probe and can now do 13C experiments. What are the
typical parameters for running a decoupled 13C-NMR? (PW, DE, AQ, DP, BB or CW,
etc.) The 45 degree PW for 1H is 5.7us. Any help here would be greatly
appreciated.
Mike Mosher
Michael D. Mosher
Department of Chemistry
University of Nebraska
Kearney, NE 68849-1150
mosherm@platte.unk.edu
Ph: (308) 865-8491
FAX: (308) 865-8157
(please write ATTN: CHEMISTRY on FAX)