Re: INADEQUATE 2D

David Naugler (dnaugler@sfu.ca)
Wed, 1 Dec 1999 11:23:31 -0800

----- Original Message -----
From: LANAIS RMN-500 <rmn500@df.uba.ar>
To: <bruker-users-mail@bloch.cchem.berkeley.edu>
Sent: December 1, 1999 3:43 PM
Subject: INADEQUATE 2D

> Dear NMR Bruker Users:
> I am interested in the INADEQUATE 2D program described in the paper:
> Investigation of 13C-13C long range couplings in natural-Abundance
> Samples by:
> A Bax, R Freeman and S.P. Kempsell, J.Magn.reson., 41, 349-353,(1980)
> "By removing the necessity of estimating tau values, the proposed
> extension of the original 13C-13C coupling experiment makes the
> application to unknown long-range coupling quite general".
> The INADEQUATE'S 2D described in the Bruker library gives
> connectivities not the Jc-c.
> Thanking for your kind attention.
>
> Dra. Dora G. de Kowalewski
>

You're supposed to look up the nJc-c's in a book somewhere. Can't remember
where. From memory these would be of the order of:

1Jc-c 135Hz
2Jc-c 35Hz
3Jc-c 2Hz

My recollection may be faulty so I welcome correction.

Dave Naugler