Interleaved Measurements : Summary

Igor Moudrakovski (igorm@ned1.sims.nrc.ca)
Tue, 1 Dec 1998 09:52:56 -0500

Thank a lot to all of you who responded to my question.
In total I've got several suggestion of general nature, reading of the
manuals was also quite educational.

Detailed solution came from Hans Foerster, Bruker Analytik GmbH -
thank you, Hans, for prompt help! I post his answer below.
Best regards

Igor
********************************************************************
Igor Moudrakovski
SIMS, NRC
Ottawa, K1A 0R6
Canada
Phone: (613) 993 5638
FAX : (613) 954 5242
********************************************************************

Reply from Hans Foerster:

attached are the files observe.incl and switchf1f2.hf.
Please look into the manual page A-59 for the parameter obschan.
(in older XWinNMR manual (95/3) this is p. 176 - I.M.)
The following parameters must be set:
swh, RG to digitise both spectra with the same parameters.
The pulse program can be rewritten as to use different receiver
and pulse phase cycles for both measurements.
Both channels must be set up in EDASP with preamps assigned.
For 2 channels, nbl must be set to 2 and a 2d file must be used
for acquisition.

with best regards

H. Foerster

;observe.incl
;sets SE451 receiver to appropriate reference frequency
#define obsf1=1u setnmr2|11^12^13
#define obsf2=1u setnmr2^11|12^13

;zg
#include <observe.incl>
10u pl1:f1
10u pl2:f2
1 ze
10u st0 ;resets aq memory to start
2 d1
obsf1 ;observe channel 1
5u setnmr2|7 ;resets preamp
1u setnmr2^7
3 3u:f1 ph1 ;aq on F1
(p1 ph1):f1
3u
d3:f1 ph0
1u adc ph31
aq
1m
1m eosc ;also check the command eoscnp if necessary
1m st ;increment aq memory
2u setnmr2|7 ;next channel on preamp
1u setnmr2^7
trigg
obsf2 ;observe F2
d1
1u
(p3 ph3):f2 ;F2 acquisition
3u
d3:f2 ph10
1u adc ph31 ;a separate receiver phase can be used
aq
1m
rcyc=2
1m st
lo to 2 times l1
100m wr #0 if #0
exit

ph0=0
ph10=0
ph1=0; 1 2 3
ph3=0 ;1 2 3
ph31=0; 1 2 3

=====================================================================
... ... Dr. Hans Foerster
. * . . Bruker Analytik GmbH
. . . . Application Lab
B R U K E R D-76287 Rheinstetten
. . . . Voice: +49-721-5161-120
. * . . Fax: +49-721-5161-297
... ... EMail: hans.foerster@bruker.de
=====================================================================