Hello BUMmers,
we have an AM400WB and an AC200 with ASPECT3000
DISR94/DISB94 and DUAL-Probe.
I want to make good HMQCs with 13C-decoupling. I can make a
good HMQC with BIRD-filter on CSE. But I have many problems
with the 13C-decoupling. The Lock breaks down and in a Invers 1H
are many artefacts. Must i have any filter ? Who can help me ?
Joerg
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Joerg Christ
Institut fuer Organische Chemie
der Justus-Liebig-Universitaet Giessen
Heinrich Buff-Ring 58
D-35392 Giessen
Telefon +49(0)641/99-34382
Telefax +49(0)641/99-34309
Joerg.Christ@org.Chemie.uni-giessen.de
http://www.uni-giessen.de/fb14/oc/nmr
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