Apodization of HMQC, HMBC, DQFPSCOSY.

From: Brian Killday (Killday@hboi.edu)
Date: Wed Jun 28 2000 - 11:24:56 PDT


Greetings all,

I have a question concerning optimal processing of 2D spectra. On our
AMX-500, we have been processing the experiments with the following
parameters (because this was how the standard parameter sets were written
when I took over the lab):

gs-HMQC and gs-HMBC: F2: WDW=sine, SSB=2, LB=0.3 F1: WDW=em, SSB=2, LB=30
(Note, this makes the cross peaks in the HMBC appear star shaped)

COSYDFTP: F2: WDW=qsine, SSB=2.5, LB=0 F1: WDW=qsine, SSB=2.5, LB=0

Do these parameters seem optimal for these experiments? Are there any good
sources containing "standard" processing parameters for various experiments?

Brian

K. Brian Killday
Research Specialist
Division of Biomedical Marine Research
Harbor Branch Oceanographic Institution
5600 U. S. 1, North
Ft. Pierce, FL 34946

Phone: 561-465-2400 ext. 456
Fax: 561-461-2221
Email: killday@hboi.edu



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