I am currently faced with a solid-state structural problem which I
think I can sort out using the 2D SECSY technique. I have tried to
implement a solid-state version of SECSY on our AMX-400
(basically replace the first 90 degree pulse on X with CP).
Although we are close, there are still some problems with the
phase cycling. I am wondering if anyone out there has a sequence
around for 2D solid-state SECSY which they could forward to me?
Thanks in advance.
Regards,
Mike
---------------------------------------------
Dr. Michael D. Lumsden
NMR Operator
Atlantic Region Magnetic Resonance Centre
Dalhousie University
Halifax, Nova Scotia, Canada, B3H 4J3
phone:(902)494-3322
FAX: (902)494-1310
email: lumsden@chem1.chem.dal.ca
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