Dear BUMmers,
We are trying to find Ruthenium 99 resonances of an AC-200
(10mm VSP) and a DRX-400 (5mm VSP). Have gone up and down about
a half a meg on both machines with [Ru(OH2)6]7 and [Ru(bipy)2(Cl2)].
So far only ring-down and a few glitches on the AC (our lab
seems to have a few guest frequencies between 9 and 10 MHz).
DE on the 200 was set to 200-300 usec and on the 400 was 100 usec.
PW/P1 was 10-20 usec with no decoupling. SW was 100,000 Hz.
Does anyone have an idea of what we are missing?
thanks,
dave scott
iowa state university
I'm not confused, I'm just well mixed.
- Robert Frost
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