CP/MAS of air sensitive samples?

Gerald Pearson (gpearson@umaxc.weeg.uiowa.edu)
Mon, 4 Oct 93 21:58:01 -0500


I'd like to try some solid-sate nmr on an air sensitive sample in a Bruker MAS
probe in our Bruker MSL-300. Has anyone done this? If so, I would appreciate
it if you would send details. Is a special rotor required? I presume that it
would be necessary to grind the sample & pack the rotor in a glove box.
--------------------------------------------------------------------
Gerald A. Pearson INTERNET: gpearson@umaxc.weeg.uiowa.edu
Chem. Dept., Univ. of Iowa VOICE: 319-335-1336
Iowa City, IA 52242-1219, USA FAX: 319-335-1270
--------------------------------------------------------------------