McMaster University - Chem3D03


Chem3D3 - Laboratory Manual


General

General Information
Laboratory Safety
Laboratory Notebook
Microscale Techniques
Check-in / Check-out

Material Safety Data Sheets (MSDS) - University of Utah open listings


Experiments

Unknowns Identification of two unknown compounds ~ all term
Expt. 1. Kinetic and Thermodynamic Control ~1.5 periods
Expt. 2. Grignard Reaction of a Protected b-Ketoester ~3 periods
Expt. 3. Synthesis of Dibenzoylmethane and Cinnamic Acid ~2 periods
Expt. 4. Synthesis of 5,5-dimethylcyclohexane-1,3-dione ~2 periods
Expt. 5. Microscale Synthesis of 4-Hydroxycoumarin ~1 period
Expt. 6. Thermal [2+4] and Photochemical [2+2] cycloaddition ~3 periods

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aug2002; nhw